new synthesis of monomeric o-amino thioaldehydes of thiophene, benzo[b]thiophene, furan and benzo[b]furan by reacting the corresponding o-azido aldehydes with hexamethyldisilathiane in neat acetonitrile and/or in methanol in the presence of hydrochloric acid at room temperature is reported.
Novel synthesis of stable furan and thiophene o-aminothioaldehydes through reaction of o-azidoaldehydes with hexamethyldisilathiane
DEGL'INNOCENTI, Alessandro;FUNICELLO, Maria;SCAFATO, Patrizia;SPAGNOLO, Piero
1996-01-01
Abstract
new synthesis of monomeric o-amino thioaldehydes of thiophene, benzo[b]thiophene, furan and benzo[b]furan by reacting the corresponding o-azido aldehydes with hexamethyldisilathiane in neat acetonitrile and/or in methanol in the presence of hydrochloric acid at room temperature is reported.File in questo prodotto:
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